反应条件
in tetrahydrofuran To a soln. of anhydrous salt is added C2H5MgBr at 20°C with stirring. The reaction mixture is left for 5 - 6 h at room temp.; decantation, washing with THF, water and ethanol; electron diffraction;
参考文献
Alphonse, P.; Galletti, D.; Ramalanjaona, M.; Mauret, P.
Journal de Chimie Physique et de Physico-Chimie Biologique, 1989 , vol. 86, # 3 p. 491 - 506
