in water an aq. soln. of AgNO3 is added dropwise to a stirred aq. soln. of KBrO3under reflux over 3 min, refluxed for 5 min; cooled to room temp., the ppt. is filtd., washed eith cooled distilled water, then with acetone, dried;
Chamot, E. M.; Mason, C. W.
Mikrochemie, 1928 , vol. 6, p. 82 - 91
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Gmelin Handbook: Ag: MVol.B2, 7.14, page 171 - 172