反应条件
hydrogen fluoride in neat (no solvent)
byproducts: NF3; CsF and NF4SbF6 loading in the drybox, dry HF adding on the vacuum line, stirring for 15 min at 25°C, cooling to -78°C, NF4HF2 soln. filtering, WF6 condensing at -196°C onto the soln., warming to ambient temp., volatiles removing; identified by elem. anal., IR, NMR and Raman spectra;
参考文献
Wilson, William W.; Christe, Karl O.
Inorganic Chemistry, 1982 , vol. 21, p. 2091 - 2094
