反应条件
sulfane was condesed on SbCl5 at -196°C, heated at 100°C to initiate the reaction; fractionation through a series of traps at -6, -45, -78, -112 and -196°C in vac., a -45°C trap contained the product;
参考文献
Thrasher, Joseph S.; Hosmane, Narayan S.; Naurer, Donald E.; Clifford, Alan F.
Inorganic Chemistry, 1982 , vol. 21, p. 2506 - 2508