in neat (no solvent)
distillation of O2F2 into boron silicate glass in vacuum; cooling at 90°K; addn. of equimolar amount ClF at 119 - 140°K; cooling at 90°K; evacuation of F2 and Cl2;;
参考文献
Streng, A. G.; Grosse, A. V.
Advances in Chemistry Series, 1962 , vol. 36, p. 159 - 165
Show Details
Gmelin Handbook: Cl: SVol.B2, 124, page 578 - 579
