in neat (no solvent)
detailed description of apparatus given; introduction of HF to cooled S4N4/CuO mixture (cooling mixture); heating (2h/100°C); cooled (liquid air or CO2/alc.);; frationation;;
参考文献
Ruff, O.; Thiel, C.
Ber., 1905 , vol. 38, p. 549 - 553
Soell, J.
FIAT Review, Naturforschung und Medizin in Deutschland 1939- 1946, fuer Deutschland bestimmte Ausgabe der FIAT Review of German Science, Dieterichsche Verlagsbuchhandlung, Wiesbaden, Bd. 23, S. 192
in neat (no solvent)
introduction of HF into mixture at common temps.;;
参考文献
Soell, J.
FIAT Review, Naturforschung und Medizin in Deutschland 1939- 1946, fuer Deutschland bestimmte Ausgabe der FIAT Review of German Science, Dieterichsche Verlagsbuchhandlung, Wiesbaden, Bd. 23, S. 192
in benzene
20°C, 48 h, in sealed tube; further products: S8 and unidentified products;
参考文献
Kaz'mina, N. B.; Knunyants, I. L.; Mysov, E. I.; Kuz'yants, G. M.
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1978 , p. 142 - 149
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1978 , p. 163 - 171
C. A., 1978 , vol. 88, p. 151687
ClSO2F (sulfuryl chloride fluoride) in not given
SO2ClF and ClF were condensed onto (SCl)2NAsF6, mixt. was warmed to room temp. with srirring, 5 h; volatiles were removed, products were not isolated; products were analized by IR;
参考文献
Brooks, Wendell V. F.; MacLean, Gregory K.; Passmore, Jack; White, Peter S.; Wong, Chi-Ming
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1983 , p. 1961 - 1968
