1-甲基-2,2-二苯基乙烯合成路线 (共 153 条)
反应条件
NiCl2((PPh3)P)2 in diethyl ether; benzene
15 h; Ambient temperature;
参考文献
Ni, Zhi-Jie; Luh, Tien-Yau
Journal of the Chemical Society, Chemical Communications, 1987 , # 20 p. 1515 - 1517
参考文献
Huisgen, Rolf; Rapp, Jochen
Journal of the American Chemical Society, 1987 , vol. 109, # 3 p. 902 - 903
反应条件
in tetrahydrofuran; diethyl ether
T=20°C; Cycloaddition;
参考文献
Huisgen, Rolf; Kalvinsch, Ivars; Li, Xingya; Mloston, Grzegorz
European Journal of Organic Chemistry, 2000 , # 9 p. 1685 - 1694
反应条件
pyridine in methanol
T=5°C; Irradiation;
参考文献
Kitamura, Tsugio; Kobayashi, Shinjiro; Taniguchi, Hiroshi
Journal of the American Chemical Society, 1986 , vol. 108, # 10 p. 2641 - 2645
反应条件
[bmim][SbF6]; scandium tris(trifluoromethanesulfonate) in water-d2
T=85°C; 4 h; Title compound not separated from byproducts.;
参考文献
Yoon, Mi Young; Kim, Jin Hong; Choi, Doo Seoung; Shin, Ueon Sang; Lee, Jin Yong; Song, Choong Eui
Advanced Synthesis and Catalysis, 2007 , vol. 349, # 10 p. 1725 - 1737
反应条件
water; acetic acid; bis-triphenylphosphine-palladium(II) chloride
T=20°C; 6 h;
参考文献
Zeng, Hanxiang; Hua, Ruimao
Journal of Organic Chemistry, 2008 , vol. 73, # 2 p. 558 - 562
反应条件
N,N,N',N',N'',N''-hexamethylphosphoric triamide in diethyl ether; hexane
T=20°C; 1 h; Further byproducts given. Yields of byproduct given;
参考文献
Tanaka, Jiro; Nojima, Masatomo; Kusabayashi, Shigekazu
Journal of the American Chemical Society, 1987 , vol. 109, # 11 p. 3391 - 3397
反应条件
dimethyl acetylenedicarboxylate in tetrahydrofuran
T=-45°C;
参考文献
Huisgen, Rolf; Xingya, Li
Heterocycles, 1983 , vol. 20, # 12 p. 2363 - 2368
反应条件
lithium hydride; zinc(II) iodide; tetrakis(triphenylphosphine) palladium(0)
1.) THF, room temp., 3 h; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Gao, Yuan; Harada, Kousuke; Hata, Takeshi; Urabe, Hirokazu; Sato, Fumie
Journal of Organic Chemistry, 1995 , vol. 60, # 2 p. 290 - 291
反应条件
lithium-di-t-butylbiphenyl in tetrahydrofuran
T=-70°C; 1 h;
参考文献
Maercker, Adalbert; Boes, Benno; Hajgholipour, Mohammad Taghi
Journal of Organometallic Chemistry, 1998 , vol. 566, # 1-2 p. 143 - 149