1-异丙基-1,2,3,4-四氢异喹啉合成路线 (共 18 条)
反应条件
C21H21ClIrNO2 in 2,2,2-trifluoroethanol 3 h; RefluxInert atmosphere;
参考文献
Angewandte Chemie - International Edition, , vol. 52, # 27 p. 6983 - 6987
Ross. Khim. Zh., , vol. 125, # 27 p. 7121 - 7125,5
反应条件
C21H21ClIrNO2 in 2,2,2-trifluoroethanol 3 h; RefluxInert atmosphere;
参考文献
Angewandte Chemie - International Edition, , vol. 52, # 27 p. 6983 - 6987
Ross. Khim. Zh., , vol. 125, # 27 p. 7121 - 7125,5
反应条件
C21H21ClIrNO2 in tetrahydrofuran; 2,2,2-trifluoroethanol 20 h; Inert atmosphere;
参考文献
Wu, Jianjun; Talwar, Dinesh; Johnston, Steven; Yan, Ming; Xiao, Jianliang
Angewandte Chemie - International Edition, 2013 , vol. 52, # 27 p. 6983 - 6987
Ross. Khim. Zh., 2013 , vol. 125, # 27 p. 7121 - 7125,5
反应条件
C21H21ClIrNO2 in 2,2,2-trifluoroethanol 3 h; RefluxInert atmosphere;
参考文献
Angewandte Chemie - International Edition, , vol. 52, # 27 p. 6983 - 6987
Ross. Khim. Zh., , vol. 125, # 27 p. 7121 - 7125,5
反应条件
C26H29ClIrNO3; hydrogen in 2,2,2-trifluoroethanol
T=20°C; P=760.051 Torr; 3 h;
参考文献
Wu, Jianjun; Barnard, Jonathan H.; Zhang, Yi; Talwar, Dinesh; Robertson, Craig M.; Xiao, Jianliang
Chemical Communications, 2013 , vol. 49, # 63 p. 7052 - 7054
反应条件
trifluorormethanesulfonic acid
T=150°C; 13 h;
参考文献
Yokoyama, Akihiro; Ohwada, Tomohiko; Shudo, Koichi
Journal of Organic Chemistry, 1999 , vol. 64, # 2 p. 611 - 617
反应条件
hydrogenchloride
8 h; Heating;
参考文献
Seebach, Dieter; Lohmann, Jean-Jacques; Syfrig, Max A.; Yoshifuji, Masaaki
Tetrahedron, 1983 , vol. 39, # 12 p. 1963 - 1974
反应条件
1: SnCl4 / 20 h / Heating
2: H2, HOAc / PtO2 / ethanol / 16 h / 2844.3 Torr
View Scheme
参考文献
Gray, Nancy M.; Cheng, Brian K.; Mick, Stephen J.; Lair, Cecelia M.; Contreras, Patricia C.
Journal of Medicinal Chemistry, 1989 , vol. 32, # 6 p. 1242 - 1248
反应条件
2,2'-azo-bisisobutyronitrile; tri-n-butyl-tin hydride in benzene
Yields of byproduct given;
参考文献
Tomaszewski; Warkentin
Tetrahedron Letters, 1992 , vol. 33, # 16 p. 2123 - 2126
反应条件
2,2'-azo-bisisobutyronitrile; tri-n-butyl-tin hydride in benzene
4 h; Heating; Yield given;
参考文献
Tomaszewski, Miroslaw J.; Warkentin, John; Werstiuk, Nick H.
Australian Journal of Chemistry, 1995 , vol. 48, # 2 p. 291 - 322