4-(1-甲乙基)苯丙醛合成路线 （共 12 条）
参考文献
Scriabine,I.
Bulletin de la Societe Chimique de France, 1961 , p. 1194 - 1198
反应条件
[3-{(1−3-η3)-1,2,3-trimethylallyl}-1,2-(CH3)2-3,1,2-closo-RhC2B9H9]; hydrogen in carbon dioxide
T=60°C; P=22801.5 Torr; 3 - 5 h; Autoclaveliquid CO2; Reagent/catalyst; regioselective reaction;
参考文献
Galkin, Konstantin I.; Lubimov, Sergey E.; Godovikov, Ivan A.; Dolgushin, Fedor M.; Smolyakov, Alexander F.; Sergeeva, Elena A.; Davankov, Vadim A.; Chizhevsky, Igor T.
Organometallics, 2012 , vol. 31, # 17 p. 6080 - 6084
反应条件
sodium acetate; pyridinium chlorochromate in dichloromethane
T=10°C; 2.5 h;
参考文献
Vig, O. P.; Bari, S. S.; Singh, K.; Dua, D. M.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1981 , vol. 20, # 7 p. 619 - 620
反应条件
diisobutylaluminium hydride in n-heptane
参考文献
Ho, Tse-Lok
Synthetic Communications, 1981 , vol. 11, # 8 p. 605 - 608
反应条件
1: 89.5 percent / tetrahydrofuran / Ambient temperature
2: 62.5 percent / iodine / 30 h / 170 - 180 °C
3: diisobutylaluminum hydride / heptane
View Scheme
参考文献
Ho, Tse-Lok
Synthetic Communications, 1981 , vol. 11, # 8 p. 605 - 608
反应条件
1: 62.5 percent / iodine / 30 h / 170 - 180 °C
2: diisobutylaluminum hydride / heptane
View Scheme
参考文献
Ho, Tse-Lok
Synthetic Communications, 1981 , vol. 11, # 8 p. 605 - 608
反应条件
sulfuric acid in ethanol
Heating;
参考文献
Scriabine,I.
Bulletin de la Societe Chimique de France, 1961 , p. 1194 - 1198
反应条件
1: 45 percent / cuprous chloride / tetrahydrofuran / 0.83 h / Ambient temperature
2: 60 percent / LiAlH4 / diethyl ether / 10 h
3: 60 percent / pyridinium chlorochromate, NaOAc / CH2Cl2 / 2.5 h / 10 °C
View Scheme
参考文献
Vig, O. P.; Bari, S. S.; Singh, K.; Dua, D. M.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1981 , vol. 20, # 7 p. 619 - 620
反应条件
boron trifluoride diethyl etherate; titanium tetrachloride
T=-30°C;
参考文献
Scriabine,I.
Bulletin de la Societe Chimique de France, 1961 , p. 1194 - 1198
反应条件
Kochen des erhaltenen Acetals mit Salzsaeure;
参考文献
Bert
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1928 , vol. 186, p. 700
