2-氯-5-硝基三氟甲苯合成路线 （共 53 条）
反应条件
1: SnCl2; aqueous HCl 2: NaNO2; aqueous H2SO4 / anschliessendes Erwaermen mit wss. H2SO4 unter Einleiten von Wasserdampf View Scheme
参考文献
Mooradian et al.
Journal of the American Chemical Society, 1951 , vol. 73, p. 3470
反应条件
1: 83 percent / K2CO3 / N,N-dimethyl-acetamide / 12 h / 100 °C 2: 84 percent / hydrazine monohydrate / 10 percent Pd/C / ethanol / 2 h / Heating View Scheme
参考文献
Yang, Chin-Ping; Chen, Ruei-Shin; Chen, Kuei-Hung; Chen, Ya-Ping
Journal of the Chinese Chemical Society, 2002 , vol. 49, # 5 p. 927 - 934
反应条件
1: With potassium carbonate 2: With 10 palladium on activated charcoal; hydrazine
参考文献
Hsiao, Sheng-Huei; Liou, Guey-Sheng; Kung, Yi-Chun; Chang, Yu-Ming
Journal of Polymer Science, Part A: Polymer Chemistry, 2010 , vol. 48, # 13 p. 2798 - 2809
反应条件
potassium carbonate in N,N-dimethyl-formamide T=130°C; 24 h;
参考文献
Xu, Wenzong; Zhang, Yingying; Hu, Yuan; Lu, Bo; Cai, Tongming
Asian Journal of Chemistry, 2012 , vol. 24, # 9 p. 3976 - 3980
反应条件
tetrakis(triphenylphosphine) palladium(0); potassium carbonate in 1,4-dioxane; water Suzuki-Miyaura coupling; 24 h; Heating;
参考文献
Gray; Andrews; Hook; Kitteringham; Voyle
Tetrahedron Letters, 2000 , vol. 41, # 32 p. 6237 - 6240
参考文献
Frazier,T.C. et al.
Journal of Organic Chemistry, 1961 , vol. 26, p. 2223 - 2225
反应条件
1: SnCl2; aqueous HCl 2: NaNO2; aqueous H2SO4 / anschliessendes Erwaermen mit wss. H2SO4 unter Einleiten von Wasserdampf View Scheme
参考文献
Journal of the American Chemical Society, , vol. 73, p. 3470
参考文献
Journal of Chemical Research - Part S, , # 2 p. 69 - 71
参考文献
Hepworth,J.D. et al.
Synthesis, 1974 , p. 874 - 876
反应条件
sodium hydroxide; tetraethylammonium chloride in methanol; water
参考文献
Bayer Aktiengesellschaft
Patent: US4225731 A1, 1980 ;
