(3,4-二甲氧基苯基)丙酮合成路线 （共 58 条）
反应条件
1: NaH / dimethylformamide / 1.) 0 deg C, 1 h; 2.) RT, 1 h; 3.) 0 deg C, 6 h; 4.) RT, 18 h 2: cc. HCl / methanol / Heating View Scheme
参考文献
Chemistry Letters, , p. 1597 - 1598
反应条件
1: 90 percent / NaBH4 / ethanol / 6 h / Ambient temperature 2: NaH / dimethylformamide / 1.) 0 deg C, 1 h; 2.) RT, 1 h; 3.) 0 deg C, 6 h; 4.) RT, 18 h 3: cc. HCl / methanol / Heating View Scheme
参考文献
Chemistry Letters, , p. 1597 - 1598
反应条件
boron trifluoride diethyl etherate; acetic acid; hydrazine 1.) EtOH, H2O, 2.) acetone, RT, 24 h; Yield given. Multistep reaction;
参考文献
Journal of Organic Chemistry, , vol. 50, # 7 p. 1019 - 1026
反应条件
1: 1.) t-BuLi / 1.) THF, pentane, from -78 deg C to -25 deg C, 1.5 h, 2.) from -78 deg C to RT, 2 h 2: 1.) hydrazine, glacial acetic acid, 2.) BF3*Et2O / 1.) EtOH, H2O, 2.) acetone, RT, 24 h View Scheme
参考文献
Journal of Organic Chemistry, , vol. 50, # 7 p. 1019 - 1026
反应条件
methanol; diethyl ether
参考文献
Monatshefte fuer Chemie, , vol. 53/54, p. 435
反应条件
Neutral lead acetate
参考文献
Yakugaku Kenkyu, , vol. 30, p. 185,191
Chem.Abstr., , p. 1517
反应条件
iodo-alcohol Einw. von AgNO3 oder HgO auf das gebildete Jodhydrin;
参考文献
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, , vol. 141, p. 597
Bulletin de la Societe Chimique de France, , vol. <4> 3, p. 735
反应条件
chromium(VI) oxide; sulfuric acid
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 1548 - 1551
参考文献
Yakugaku Zasshi, , vol. 79, p. 1335,1337
Chem.Abstr., , p. 4475
参考文献
Yakugaku Zasshi, , vol. 79, p. 1335,1337
Chem.Abstr., , p. 4475
