(3,4-二甲氧基苯基)丙酮合成路线 （共 58 条）
反应条件
KBrO3; palladium 10 on activated carbon in tetrahydrofuran; water T=65°C; Wacker Oxidation;
参考文献
Kulkarni, Mukund G.; Shaikh, Yunnus B.; Borhade, Ajit S.; Chavhan, Sanjay W.; Dhondge, Attrimuni P.; Gaikwad, Dnyaneshwar D.; Desai, Mayur P.; Birhade, Deekshaputra R.; Dhatrak, Nagorao R.
Tetrahedron Letters, 2013 , vol. 54, # 19 p. 2293 - 2295
反应条件
L-Selectridereg; in tetrahydrofuran 0.5 h;
参考文献
Mourad, M. Soubei; Varma, Rajender S.; Kabalka, George W.
Synthesis, 1985 , # 6/7 p. 654 - 656
反应条件
in tetrahydrofuran T=0°C;
参考文献
Gerritz; Smith; Nanthakumar; Uehling; Cobb
Organic letters, 2000 , vol. 2, # 25 p. 4099 - 4102
参考文献
Ube Industries, Ltd.
Patent: US4638094 A1, 1987 ;
反应条件
1: 62.7 percent / butylamine / 168 h 2: 47 percent / reduced iron, nickel chloride hexahydrate, concd. hydrochloric acid / toluene; H2O / 4 h / Heating View Scheme
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 25, # 7.2 p. 1332 - 1337
Zhurnal Organicheskoi Khimii, , vol. 25, # 7 p. 1477 - 1482
反应条件
acetic acid; zinc T=100°C; 1 h;
参考文献
Tamura, Yasumitsu; Choi, Hong Dae; Mizutani, Masako; Ueda, Yuko; Ishibashi, Hiroyuki
Chemical and Pharmaceutical Bulletin, 1982 , vol. 30, # 10 p. 3574 - 3579
反应条件
indium; chloro-trimethyl-silane T=25°C; Reduction; Addition; 3.5 h;
参考文献
Yadav; Subba Reddy; Srinivas; Ramalingam
Synlett, 2000 , # 10 p. 1447 - 1449
反应条件
1: hydrolysis 2: 21 percent / R4 medium; thiostrepton; Streptomyces coelicolor CH999/pIJ5660 recombinant strain / methanol; dimethylformamide; glycerol / 96 h / 30 °C View Scheme
参考文献
Angewandte Chemie - International Edition, , vol. 44, # 7 p. 1121 - 1125
反应条件
oxygen; bornyl acetate; palladium dichloride in isobutyramide; water T=60°C; P=7600.51 Torr; 7 h;
参考文献
Advanced Synthesis and Catalysis, , vol. 352, # 9 p. 1533 - 1538
反应条件
[Pd(η3-1-Ph-allyl)(μ-Cl)]2; (Mor-DalPhos); caesium carbonate T=90°C; 16 h; Inert atmospheresealed vial;
参考文献
Hesp, Kevin D.; Lundgren, Rylan J.; Stradiotto, Mark
Journal of the American Chemical Society, 2011 , vol. 133, # 14 p. 5194 - 5197
