poly(ethylene glycol) or poly(vinylpyrrolidone) in water High Pressure; for urchinlike structures soln. of mixt. sealed in autoclave, heated to 110 or 130 °C (1 °C/min), maintained at 130 °C for 16 h; for sisalike structures polymer added, heated in autoclave at 110(PEG) or 90 °C (PVP) for 16 h;
Mahant, S. D.
Journal of the Indian Chemical Society, 1929 , vol. 6, p. 706
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Bhatnagar, S. S.; Sharma, R. K.; Mitra, N. G.
Journal of the Indian Chemical Society, 1928 , vol. 5, p. 382
in hydrogen fluoride byproducts: Br2; HF (liquid); excess of BrF5, standing in Kel-F tube for 3-5 d; distn. off of BrO2F (vac.; trap at -48°C); product mixt. (10percent KBrF4O) not sepd., detd. by Raman spectroscopy;
参考文献
Gillespie, Ronald J.; Spekkens, Paul
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1976 , p. 2391 - 2396
Lenher, V.; Kao, C. H.
Journal of the American Chemical Society, 1926 , vol. 48, p. 1554 - 1554
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Lenher, V.; Kao, C. H.
Journal of the American Chemical Society, 1926 , vol. 48, p. 1552
