1,2,3,3,4,5,6,6-八氟-1,4-环己二烯合成路线 （共 34 条）
反应条件
bromine trifluoride; SbF5
T=60 - 120°C; Kochen des Reaktionsprodukts mit Zinkstaub und Aethanol;
参考文献
McBee; Lindgren; Ligett
Industrial and Engineering Chemistry, 1947 , vol. 39, p. 378,379
Show Details
Purdue Research Found.
Patent: US2498891 , 1945 ;
Full Text Show Details
Purdue Research Found.
Patent: US2432997 , 1945 ;
Full Text Show Details
Purdue Research Found.
Patent: US2586364 , 1946 ;
反应条件
bromine trifluoride; SbF5
T=60 - 120°C; Kochen des Reaktionsprodukts mit Zinkstaub und Aethanol;
参考文献
McBee; Lindgren; Ligett
Industrial and Engineering Chemistry, 1947 , vol. 39, p. 378,379
Show Details
Purdue Research Found.
Patent: US2498891 , 1945 ;
Full Text Show Details
Purdue Research Found.
Patent: US2432997 , 1945 ;
Full Text Show Details
Purdue Research Found.
Patent: US2586364 , 1946 ;
反应条件
iodine heptafluoride; acetonitrile in 1,1,1,3,3-pentafluoropropane
T=-70 - 0°C;
参考文献
Frohn, Hermann-Josef; Bardin, Vadim V.
Journal of Fluorine Chemistry, 2010 , vol. 131, # 10 p. 1000 - 1006
反应条件
iodine heptafluoride in 1,1,1,3,3-pentafluoropropane
T=-60°C; 1 h;
参考文献
Frohn, Hermann-Josef; Bardin, Vadim V.
Journal of Fluorine Chemistry, 2010 , vol. 131, # 10 p. 1000 - 1006
反应条件
tetrafluoroammonium tetrafluoroborate in hydrogen fluoride
12 h; Ambient temperature; Title compound not separated from byproducts;
参考文献
Schack, Carl J.; Christe, Karl O.
Journal of Fluorine Chemistry, 1981 , vol. 18, p. 363 - 374
反应条件
iodine heptafluoride; acetonitrile in 1,1,1,3,3-pentafluoropropane
T=-60 - -40°C;
参考文献
Frohn, Hermann-Josef; Bardin, Vadim V.
Journal of Fluorine Chemistry, 2010 , vol. 131, # 10 p. 1000 - 1006
反应条件
1: With tetramethyl-ammonium fluoride in 1,1,1,3,3-pentafluoropropane
T=-70 - -30°C; 0.416667 h;
2: With iodine heptafluoride in 1,1,1,3,3-pentafluoropropane
T=-30 - 0°C; 3 h;
参考文献
Frohn, Hermann-Josef; Bardin, Vadim V.
Journal of Fluorine Chemistry, 2010 , vol. 131, # 10 p. 1000 - 1006
反应条件
iodine heptafluoride; acetonitrile in 1,1,1,3,3-pentafluoropropane
T=-70 - -40°C; 1.5 h;
参考文献
Frohn, Hermann-Josef; Bardin, Vadim V.
Journal of Fluorine Chemistry, 2010 , vol. 131, # 10 p. 1000 - 1006
反应条件
iodine heptafluoride; acetonitrile in 1,1,1,3,3-pentafluoropropane
T=-60 - 6°C;
参考文献
Frohn, Hermann-Josef; Bardin, Vadim V.
Journal of Fluorine Chemistry, 2010 , vol. 131, # 10 p. 1000 - 1006
反应条件
potassium hydroxide; silicone antifoam agent in water
0.75 h; Heating; Yield given. Yields of byproduct given;
参考文献
Coe, Paul L.; Mott, Andrew W.; Tatlow, John Colin
Journal of Fluorine Chemistry, 1982 , vol. 20, p. 167 - 172
