N-正辛基-3,4-噻吩二甲酰亚胺合成路线 （共 8 条）
反应条件
N-bromosuccinmide in sulfuric acid; trifluoroacetic acid T=20°C;
参考文献
Zou, Yingping; Najari, Ahmed; Berrouard, Philippe; Beaupre, Serge; Reda Aich, Badrou; Tao, Ye; Leclerc, Mario
Journal of the American Chemical Society, 2010 , vol. 132, # 15 p. 5330 - 5331
反应条件
N-bromosuccinmide in N,N-dimethyl-formamide
参考文献
Berrouard, Philippe; Grenier, Francois; Pouliot, Jean-Remi; Gagnon, Eric; Tessier, Christian; Leclerc, Mario
Organic Letters, 2011 , vol. 13, # 1 p. 38 - 41
反应条件
1: thiophene-3,4-dicarboxylic acid With acetic anhydride
T=140°C;
2: n-Octylamine in toluene
24 h; Reflux;
3: With thionyl chloride
4 h; Reflux;
参考文献
Zou, Yingping; Najari, Ahmed; Berrouard, Philippe; Beaupre, Serge; Reda Aich, Badrou; Tao, Ye; Leclerc, Mario
Journal of the American Chemical Society, 2010 , vol. 132, # 15 p. 5330 - 5331
反应条件
thionyl chloride
3 h; Heating;
参考文献
Nielsen, Christian B.; Bjornholm, Thomas
Organic Letters, 2004 , vol. 6, # 19 p. 3381 - 3384
反应条件
1: 86 percent / Ac2O / 140 °C
2: 85 percent / toluene / 24 h / Heating
3: 79 percent / SOCl2 / 3 h / Heating
View Scheme
参考文献
Nielsen, Christian B.; Bjornholm, Thomas
Organic Letters, 2004 , vol. 6, # 19 p. 3381 - 3384
反应条件
1: 85 percent / toluene / 24 h / Heating
2: 79 percent / SOCl2 / 3 h / Heating
View Scheme
参考文献
Nielsen, Christian B.; Bjornholm, Thomas
Organic Letters, 2004 , vol. 6, # 19 p. 3381 - 3384
反应条件
1: 74 percent / KOH / ethane-1,2-diol / Heating
2: 86 percent / Ac2O / 140 °C
3: 85 percent / toluene / 24 h / Heating
4: 79 percent / SOCl2 / 3 h / Heating
View Scheme
参考文献
Nielsen, Christian B.; Bjornholm, Thomas
Organic Letters, 2004 , vol. 6, # 19 p. 3381 - 3384
参考文献
Zhang, Yong; Hau, Steven K.; Yip, Hin-Lap; Sun, Ying; Acton, Orb; Jen, Alex K.-Y.
Chemistry of Materials, 2010 , vol. 22, # 9 p. 2696 - 2698
