(2-噻吩-2-苯基)甲醇合成路线 （共 3 条）
反应条件
lithium aluminium tetrahydride in tetrahydrofuran T=20°C; 0.666667 h;
参考文献
Bancerz, Mathew; Huck, Lawrence A.; Leigh, William J.; Mladenova, Gabriela; Najafian, Katayoun; Zeng, Xiaofeng; Lee-Ruff, Edward
Journal of Physical Organic Chemistry, 2010 , vol. 23, # 12 p. 1202 - 1213
反应条件
1: tetrakis(triphenylphosphine) palladium(0); sodium carbonate / ethanol; benzene / Inert atmosphere; Reflux 2: lithium aluminium tetrahydride / tetrahydrofuran / 0.67 h / 20 °C View Scheme
参考文献
Journal of Physical Organic Chemistry, , vol. 23, # 12 p. 1202 - 1213
反应条件
1: polyphosphoric acid / dichloromethane / 0.07 h / 120 °C
2: N-bromosuccinmide / tetrachloromethane / 2.5 h / Reflux; Irradiation
3: water; silver nitrate / acetone / 0.17 h
4: Inert atmosphere; UV-irradiation
View Scheme
参考文献
Bancerz, Mathew; Huck, Lawrence A.; Leigh, William J.; Mladenova, Gabriela; Najafian, Katayoun; Zeng, Xiaofeng; Lee-Ruff, Edward
Journal of Physical Organic Chemistry, 2010 , vol. 23, # 12 p. 1202 - 1213
