5,5,5-三氟戊-1-烯-4-醇合成路线 (共 8 条)
反应条件
indium in water
15 h; Ambient temperature;
参考文献
Loh, Teck-Peng; Li, Xu-Ran
Tetrahedron, 1999 , vol. 55, # 17 p. 5611 - 5622
反应条件
indium in water
15 h; Ambient temperature;
参考文献
Loh, Teck-Peng; Li, Xu-Ran
Tetrahedron, 1999 , vol. 55, # 17 p. 5611 - 5622
反应条件
indium in water
T=20°C; 5 h;
参考文献
Harthong, Steven; Billard, Thierry; Langlois, Bernard R.
Synthesis, 2005 , # 13 art. no. Z12005SS, p. 2253 - 2263
反应条件
zinc(II) iodide in 1,4-dioxane
参考文献
Kubota, Toshio; Iijima, Masahiro; Tanaka, Tatsuo
Tetrahedron Letters, 1992 , vol. 33, # 10 p. 1351 - 1354
反应条件
zinc in tetrahydrofuran
2 h; ultrasonic irradiation;
参考文献
Ishikawa, Nobuo; Koh, Moon Gyu; Kitazume, Tomoya; Choi, Sam Kwon
Journal of Fluorine Chemistry, 1984 , vol. 24, p. 419 - 430
反应条件
zinc dibromide in diethyl ether
2 h;
参考文献
Harthong, Steven; Billard, Thierry; Langlois, Bernard R.
Synthesis, 2005 , # 13 art. no. Z12005SS, p. 2253 - 2263
反应条件
hexane; diisobutylaluminium hydride; ethylene dibromide; zinc
1.) CH2Cl2, -78 deg C, 1 h, 2.) CH2Cl2, 40 deg C, 4 h; Yield given. Multistep reaction;
参考文献
Ishihara; Hayashi; Yamanaka
Tetrahedron Letters, 1993 , vol. 34, # 36 p. 5777 - 5780
反应条件
n-butyllithium; 1,8-diiodo-naphthalene; di-n-butyldichlorostannane
2.) PhMe, r.t., 70 h; Yield given. Multistep reaction;
参考文献
Asao; Liu; Maruoka
Angewandte Chemie - International Edition in English, 1997 , vol. 36, # 22 p. 2507 - 2509