1: With hydrogenchloride; sodium nitrite T=0°C; 0.25 h; 2: With potassium iodide T=20°C; 12 h; Further stages.;
参考文献
Takahashi, Tamotsu; Li, Yanzhong; Stepnicka, Petr; Kitamura, Masanori; Liu, Yanjun; Nakajima, Kiyohiko; Kotora, Martin
Journal of the American Chemical Society, 2002 , vol. 124, # 4 p. 576 - 582
n-butyllithium; iodine; diisopropylamine 1.) THF, hexane, -78 grad C, 30 min, 2.) THF, hexane, -78 grad C, then slowly allowed to warm to room temperature overnight.; Yield given. Multistep reaction;
参考文献
Gribble, Gordon W.,; Saulnier, Mark G.
Tetrahedron Letters, 1980 , vol. 21, p. 4137 - 4140
