2-甲基-5-硝基苯甲酸甲酯合成路线 （共 27 条）
参考文献
Recueil des Travaux Chimiques des Pays-Bas, , vol. 20, p. 169
参考文献
Recueil des Travaux Chimiques des Pays-Bas, , vol. 20, p. 169
参考文献
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, , vol. 23, # 11 p. 1098 - 1102
参考文献
Recueil des Travaux Chimiques des Pays-Bas, , vol. 20, p. 169
反应条件
N-bromosuccinmide; dibenzoyl peroxide in tetrachloromethane 34 h; Reflux;
参考文献
THE BOARD OF TRUSTEES OF THE UNIVERSITY OF ILLINOIS; PURDUE RESEARCH FOUNDATION
Patent: US2011/269834 A1, 2011 ;
Location in patent: Page/Page column 29 ;
反应条件
dibenzoyl peroxide in tetrachloromethane; water
参考文献
MERCK SHARP and DOHME LTD.
Patent: EP514133 A1, 1992 ;
EP 0514133 A1
反应条件
1: 94 percent / H2 / 10percent Pd/C / ethanol / 2 h / 1520 - 2280 Torr 2: 64 percent / 5.4 volpercent H2SO4, aq. NaNO2 / 0.5 h / Heating View Scheme
参考文献
Bird; Bruneau; Crawley; Edwards; Foster; Girodeau; Kingston; McMillan
Journal of Medicinal Chemistry, 1991 , vol. 34, # 7 p. 2176 - 2186
参考文献
van Scherpenzeel
Recueil des Travaux Chimiques des Pays-Bas, 1901 , vol. 20, p. 169
反应条件
1: N-bromosuccinimide (NBS), benzoyl peroxide / CCl4 / 20 h / Heating 2: NaOH, tricaprylmethylammonium chloride / CH2Cl2; H2O / 5 h / Ambient temperature 3: 82 percent / aq. 4 N KOH / methanol / 4 h / Ambient temperature View Scheme
参考文献
Wakselman; Mazaleyrat; Xie; Montagne; Vilain; Reboud-Ravaux
European Journal of Medicinal Chemistry, 1991 , vol. 26, # 7 p. 699 - 707
反应条件
1: N-bromosuccinmide; dibenzoyl peroxide / tetrachloromethane / 12 h / 80 °C 2: ammonia / methanol / 2 h / Reflux View Scheme
参考文献
Fu, Liqiang; Liu, Xin; Ling, Chenyu; Cheng, Jianjun; Guo, Xingsheng; He, Huili; Ding, Shi; Yang, Yushe
Bioorganic and Medicinal Chemistry Letters, 2012 , vol. 22, # 2 p. 814 - 819
