1-(6-甲氧基-2-萘甲基)乙醇合成路线 (共 6 条)
反应条件
hydrogen; palladium on activated charcoal; 5 percent palladium-carbon in tetrahydrofuran
参考文献
Xie, Bao-Han; Xia, Chun-Gu; Lu, Shi-Jie; Chen, Ke-Jun; Kou, Yuan; Yuan-Qi, Yin
Tetrahedron Letters, 1998 , vol. 39, # 40 p. 7365 - 7368
反应条件
samarium in methanol T=20°C; reductive coupling; 20 h;
参考文献
Tetrahedron Letters, , vol. 41, # 20 p. 3793 - 3796
反应条件
lithium aluminium tetrahydride; TiI4 in tetrahydrofuran T=-5°C; 0.5 h;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , # 13 p. 1771 - 1774
反应条件
1: 68 percent / n-BuLi / tetrahydrofuran; hexane / 1.5 h / -78 - -70 °C 2: 91 percent / sodium borohydride / tetrahydrofuran; ethanol / 3 h / 20 °C View Scheme
参考文献
Bioorganic and Medicinal Chemistry, , vol. 12, # 16 p. 4313 - 4336
反应条件
n-butyllithium 1.) Et2O, hexane, 1 h, 2.) 2 h; Multistep reaction;
参考文献
Tetrahedron, , vol. 53, # 21 p. 7101 - 7118
反应条件
ammonium cerium(IV) nitrate in methanol 0.5 h; var. molar ratio of the oxidant; other oxidant; also anodic oxidation; sodium salt of naproxen; Product distribution;
参考文献
Journal of Pharmaceutical Sciences, , vol. 81, # 5 p. 479 - 482