2,4,6-三甲基苯磺酰氯合成路线 （共 56 条）
反应条件
chlorosulfonic acid in chloroform T=-5 - 20°C; 1 h;
参考文献
Faber, Wijnand S.; Kok, Johan; De Lange, Ben; Feringa, Ben L.
Tetrahedron, 1994 , vol. 50, # 16 p. 4775 - 4794
反应条件
2,4,6-trichloro-1,3,5-triazine; 18-crown-6 ether in acetone 20 h; Heating;
参考文献
Blotny, Grzegorz
Tetrahedron Letters, 2003 , vol. 44, # 7 p. 1499 - 1501
反应条件
2,4,6-trichloro-1,3,5-triazine; triethylamine in acetone 20 h; Heating;
参考文献
Blotny, Grzegorz
Tetrahedron Letters, 2003 , vol. 44, # 7 p. 1499 - 1501
反应条件
Reaktion mit Verbindung oder mit Natriumsalz;
参考文献
Monatshefte fuer Chemie, , vol. 34, p. 576
参考文献
Chemische Berichte, , vol. 26, p. 2942
反应条件
sodium hydroxide in dichloromethane; water T=5 - 20°C; 17 h;
参考文献
WISCONSIN ALUMNI RESEARCH FOUNDATION
Patent: WO2005/14524 A2, 2005 ;
Location in patent: Page/Page column 64 ;
参考文献
Garcia-Rio; Leis; Moreira; Norberto
Journal of Physical Organic Chemistry, 1998 , vol. 11, # 10 p. 756 - 760
反应条件
1: 1.) AlCl3 / 1.) CH2Cl2, 15 min, 2.) CH2Cl2, 18 h, RT 2: 76 percent / silica gel / CHCl3 3: 65 percent / CHCl3 / 48 h / Ambient temperature View Scheme
参考文献
Kosack, Steffen; Himbert, Gerhard
Chemische Berichte, 1987 , vol. 120, p. 71 - 78
反应条件
1: With triethylamine T=20°C; 2: With perchloric acid Neat (no solvent);
参考文献
MERCK and CO., INC.; KATZ, Jason; KNOWLES, Sandra, L.; JEWELL, James, P.; SLOMAN, David, L.; STANTON, Matthew, G.; NOUCTI, Njamkou
Patent: WO2010/17046 A1, 2010 ;
Location in patent: Page/Page column 42; 57-58 ;
WO 2010/017046 A1
反应条件
triethylamine in N,N-dimethyl-formamide T=0°C;
参考文献
BRISTOL-MYERS SQUIBB COMPANY; PRACITTO, Richard; KADOW, John, F.; BENDER, John, A.; BENO, Brett, R.; GRANT-YOUNG, Katharine; HAN, Ying; HEWAWASAM, Piyasena; NICKEL, Andrew; PARCELLA, Kyle, E.; YEUNG, Kap-Sun; CHUPAK, Louis, S.
Patent: WO2011/112186 A1, 2011 ;
Location in patent: Page/Page column 202 ;
WO 2011/112186 A1
