N-亚苄基-DL-苯基甘氨酸乙酯合成路线 （共 11 条）
反应条件
chymortypsin; water in acetonitrile 240 h; Yield given. Title compound not separated from byproducts;
参考文献
Journal of Organic Chemistry, , vol. 61, # 4 p. 1223 - 1226
反应条件
chymortypsin; water in acetonitrile 240 h; Yield given. Title compound not separated from byproducts;
参考文献
Parmar, Virinder S.; Singh, Amarjit; Bisht, Kirpal S.; Kumar, Naresh; Belokon; Kochetkov; Ikonnikov; Orlova; Tararov; Saveleva
Journal of Organic Chemistry, 1996 , vol. 61, # 4 p. 1223 - 1226
反应条件
1: NaH / dimethylformamide 2: 10percent aq. HCl / 1 h 3: 81 percent / KOH / aq. ethanol / Ambient temperature View Scheme
参考文献
European Journal of Medicinal Chemistry, , vol. 29, # 6 p. 411 - 421
反应条件
sodium sulfate; triethylamine in dichloromethane
16 h; Ambient temperature;
参考文献
Van Betsbrugge; Tourwe; Kaptein; Kierkels; Broxterman
Tetrahedron, 1997 , vol. 53, # 27 p. 9233 - 9240
反应条件
magnesium sulfate in toluene
48 h; Ambient temperature;
参考文献
Cereda; Ezhaya; Bellora; Schiavi; Sagrada; Doods; Donetti
European Journal of Medicinal Chemistry, 1994 , vol. 29, # 6 p. 411 - 421
反应条件
magnesium sulfate; triethylamine in dichloromethane
4 h; Ambient temperature;
参考文献
Duhamel, Lucette; Plaquevent, Jean-Christophe
Bulletin de la Societe Chimique de France, 1982 , vol. 2, # 1-2 p. 75 - 83
反应条件
1: 100 percent / HCl gas / 0 °C
2: 89 percent / Na2SO4, NEt3 / CH2Cl2 / 16 h / Ambient temperature
View Scheme
参考文献
Van Betsbrugge; Tourwe; Kaptein; Kierkels; Broxterman
Tetrahedron, 1997 , vol. 53, # 27 p. 9233 - 9240
反应条件
in dichloromethane
48 h; Ambient temperature;
参考文献
Bradamante, Silvia; Colombo, Silvana; Pagani, Giorgo A.; Roelens, Stefano
Helvetica Chimica Acta, 1981 , vol. 64, # 2 p. 568 - 571
反应条件
1: 88 percent / benzene / 48 h / Heating
2: 75 percent / Et3N, MgSO4 / CH2Cl2 / 4 h / Ambient temperature
View Scheme
参考文献
Duhamel, Lucette; Plaquevent, Jean-Christophe
Bulletin de la Societe Chimique de France, 1982 , vol. 2, # 1-2 p. 75 - 83
反应条件
1: 63 percent / CH2Cl2 / 48 h / Ambient temperature
2: 50 percent / CH2Cl2 / 3 h / Heating
View Scheme
参考文献
Bradamante, Silvia; Colombo, Silvana; Pagani, Giorgo A.; Roelens, Stefano
Helvetica Chimica Acta, 1981 , vol. 64, # 2 p. 568 - 571
