Ogier, J.
Ann. Chim. Phys., 1880 , vol. 20, p. 17
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Simon, J. F.
Annalen der Physik (Weinheim, Germany), 1836 , vol. 42, p. 565
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Gmelin Handbook: Br: MVol., 3.2, page 115 - 119
in sulfur dioxide
1 d; slow removal of solvent, cooling to 0°C;
参考文献
Brownridge, Scott; Cameron, T. Stanley; Passmore, Jack; Schatte, Gabriele; Way, Todd C.
Journal of the Chemical Society - Dalton Transactions, 1996 , # 12 p. 2553 - 2570
AsF5 condensed at -196°C onto a mixture of Br2 and AsBr3, warmed to -5°C, recooled to -196°C (repeated for more than 10 times); AsF3 removed at -5°C under dynamic vac.;
参考文献
Klapoetke, Thomas; Passmore, Jack; Awere, Edward G.
Journal of the Chemical Society, Chemical Communications, 1988 , # 21 p. 1426 - 1427
sulfur dioxide in water
simultaneous addition of Br2 and introduction of SO2 into a soln. of SO2 in ice water; after decoloration, SeO2 and Se are added; addition of concd. H2SO4; cooling;; washing with concd. H2SO4;;
