trimethylstannyl chloride in carbon disulfide
reaction of P4 with Br2 in CS2, followed by treatment with C(CH3)3SnCl; further products: Cl2P2Br2, ClBrP2ClBr, P2Br4, PBr3; not isolated, identified by 31P-NMR spectroscopy;
参考文献
Tattershall, Bruce W.; Kendall, Nigel L.
Polyhedron, 1994 , vol. 13, p. 1517 - 1522
in neat (no solvent)
absence of air and moisture; 150 mbar Br2, 320 mbar NO, 20°C, 30 min; fractional condensation at -65, -120, -196°C (product in -120°C trap);
Kochen des Reaktionsprodukts mit N.N-Dimethyl-anilin;
参考文献
Baker; Carlson
Journal of the American Chemical Society, 1942 , vol. 64, p. 2657,2660
Full Text Show Details
Tishler; Fieser; Wendler
Journal of the American Chemical Society, 1940 , vol. 62, p. 2866,2868
in neat (no solvent)
passing a mixture of Cl2 and Br2 over metallic Si at 700°C;; fractional distillation;;
参考文献
Schumb, W. C.; Anderson, H. H.
Journal of the American Chemical Society, 1937 , vol. 59, p. 651 - 653
Full Text View citing articles Show Details
Gmelin Handbook: Si: MVol.B, 272, page 732 - 735
