in neat (no solvent) byproducts: H2; in a quartz tube heated to 500-550°C in a stream of Br2 in Ar; sublimation at 600°C, purity 99percent;
参考文献
Golovanova, A. I.; Konstantinova, A. I.
Russian Journal of Inorganic Chemistry (Translation of Zhurnal Neorganicheskoi Khimii), 1985 , vol. 30, p. 320 - 321
Zhurnal Neorganicheskoi Khimii, 1985 , vol. 30, p. 566 - 567
in neat (no solvent) passing Br2 vapor over moderately heated Mo;; no analysis;;
参考文献
Blomstrand, C. W.
Journal fuer Praktische Chemie (Leipzig), 1861 , vol. 82, p. 434 - 434
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Gmelin Handbook: Mo: MVol., 63, page 177 - 179
Ryabov, S. A.; Alikhanyan, A. S.; Butskii, V. D.; Pervov, V. S.
Russian Journal of Inorganic Chemistry (Translation of Zhurnal Neorganicheskoi Khimii), 1989 , vol. 34, p. 570 - 573
Zhurnal Neorganicheskoi Khimii, 1989 , vol. 34, p. 1017 - 1020
in neat (no solvent) dropping (or introduction) of Br2, BrF3, SO2 into icecold SO2 (excess); finally addn. of a small excess of BrF3; left for a short time at room temp.; or react. of SO2, Br2, BrF3 (mole ratio: 3/1/1) in a water-cooled steel vessel for 1-3 d;; shaking in presence of Hg to remove of BrF3; distillation;;
参考文献
Jonas, H.
Z. Anorg. Chem., 1951 , vol. 265, p. 273 - 283
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Gmelin Handbook: S: MVol.B3, 160, page 1868 - 1870
Full Text Show Details
Jonas, H.
in: FIAT Review, Bd. 23, S. 193
