in neat (no solvent) byproducts: H2; in a quartz tube heated to 450°C in a stream of Br2 in Ar; purity 95percent;
参考文献
Golovanova, A. I.; Konstantinova, A. I.
Russian Journal of Inorganic Chemistry (Translation of Zhurnal Neorganicheskoi Khimii), 1985 , vol. 30, p. 320 - 321
Zhurnal Neorganicheskoi Khimii, 1985 , vol. 30, p. 566 - 567
Kost, M. E.; Golovanova, A. I.
Russian Journal of Inorganic Chemistry (Translation of Zhurnal Neorganicheskoi Khimii), 1977 , vol. 22, p. 460 - 460
Zhurnal Neorganicheskoi Khimii, 1977 , vol. 22, p. 832 - 833
aluminium in solid liquid Br2 was dropped into a solid mixt. of oxide and a large excess ofAl powder in one-end sealed quartz tube under Ar atm., evacuated, seale d, placed in a tabular furnace with temp. gradient from 750 to 460 K;
参考文献
Wang, Zhi-Chang; Yu, Jin
Inorganic Chemistry, 2007 , vol. 46, # 10 p. 4248 - 4255