5-溴-3,4-二氢-8-甲氧基-1(2H)-萘酮合成路线 （共 7 条）
反应条件
boron tribromide in dichloromethane 1) -70 deg C, 30 min 2) -20 deg C, 12 h;
参考文献
Pudleiner, Heinz; Laatsch, Hartmut
Liebigs Annalen der Chemie, 1990 , # 5 p. 423 - 432
反应条件
palladium 10 on activated carbon; hydrogen in ethanol T=20°C; 24 h;
参考文献
Cabrera, Elvia V.; Banerjee, Ajoy K.
Organic Preparations and Procedures International, 2010 , vol. 42, # 5 p. 499 - 502
参考文献
Chatterjee, A.; Hazra, B. G.
Tetrahedron, 1980 , vol. 36, # 17-K p. 2513 - 2520
参考文献
Abbott Laboratories
Patent: US4618683 A1, 1986 ;
US 4618683 A
反应条件
sodium peroxodisulphate; silver nitrate in water; acetone
0.333333 h; Reflux;
参考文献
Cabrera, Elvia V.; Banerjee, Ajoy K.
Organic Preparations and Procedures International, 2010 , vol. 42, # 5 p. 499 - 502
参考文献
Chatterjee, A.; Hazra, B. G.
Tetrahedron, 1980 , vol. 36, # 17-K p. 2513 - 2520
反应条件
1: 61 percent / Br2 / CHCl3 / 0.5 h / 5 °C
2: 94 percent / polyphosphoric acid / 1 h / Heating
View Scheme
参考文献
Chatterjee, A.; Hazra, B. G.
Tetrahedron, 1980 , vol. 36, # 17-K p. 2513 - 2520
