in water aq. H2O2 soln.; very slow reaction by heating on water bath with high H2O2 concn. (60percent) and finely powdered Te or pptd. Te dried at 105°C; faster reaction with pptd. Te dried by washing with alc. and ether, concd. H2O2;;
参考文献
Gilbertson, L. I.
Journal of the American Chemical Society, 1933 , vol. 55, p. 1460 - 1460
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Gmelin Handbook: Te: MVol., 80, page 287 - 289
peroxymonosulfuric acid in sulfuric acid byproducts: O2; refluxing TeO2 with 30percent H2SO4 acidic H2O2 soln. containing H2SO5;; filtration through asbestos; evapn. until crystn.; addn. of concd. HNO3; filtration through asbestos; heating; recrystn. several times from water;;
参考文献
Revzin, G. E.; Vulikh, A. I.; Zherdienko, L. P.
Patent: SU202893 , 1967 ;
C. A., 1968 , vol. 69, p. 11805
