3,3'-联吡啶-2,2'-二胺合成路线 （共 9 条）
反应条件
nickel diacetate; triphenylphosphine; sodium t-butanolate in ethylene glycol dimethyl ether
T=65°C; 17 h;
参考文献
Forst, Yves; Becker, Sandrine; Caubere, Paul
Tetrahedron, 1994 , vol. 50, # 41 p. 11893 - 11902
反应条件
sulfuric acid; zinc
T=80°C; 5 h;
参考文献
Becalski, Adam; Kaczmarek, Lukasz; Nantka-Namirski, Pawel
Bulletin of the Polish Academy of Sciences, Chemistry, 1984 , vol. 32, # 3-6 p. 105 - 114
反应条件
sodium sulfide in water
24 h;
参考文献
Becalski, Adam; Kaczmarek, Lukasz; Nantka-Namirski, Pawel
Bulletin of the Polish Academy of Sciences, Chemistry, 1984 , vol. 32, # 3-6 p. 105 - 114
反应条件
sodium sulfide in water
24 h;
参考文献
Becalski, Adam; Kaczmarek, Lukasz; Nantka-Namirski, Pawel
Bulletin of the Polish Academy of Sciences, Chemistry, 1984 , vol. 32, # 3-6 p. 105 - 114
反应条件
1: 75 percent / copper / dimethylformamide / 4 h / 100 - 110 °C
2: 53 percent / zinc, 35 percent H2SO4 / 5 h / 80 °C
View Scheme
参考文献
Becalski, Adam; Kaczmarek, Lukasz; Nantka-Namirski, Pawel
Bulletin of the Polish Academy of Sciences, Chemistry, 1984 , vol. 32, # 3-6 p. 105 - 114
反应条件
1: 68 percent / copper / dimethylformamide / 4 h / 100 - 110 °C
2: Na2S*9H2O / H2O / 24 h
View Scheme
参考文献
Becalski, Adam; Kaczmarek, Lukasz; Nantka-Namirski, Pawel
Bulletin of the Polish Academy of Sciences, Chemistry, 1984 , vol. 32, # 3-6 p. 105 - 114
反应条件
potassium hydroxide; water; bromine
参考文献
Brydowna; Wisznewski
Roczniki Chemii, 1935 , vol. 14, p. 378,381
Chem. Zentralbl., 1936 , vol. 107, # I p. 1622
反应条件
1: ethanol; NH3
2: bromine; aqueous KOH / zuletzt unter Erwaermen
View Scheme
参考文献
Brydowna; Wiszniewski
Roczniki Chemii, 1935 , vol. 15, p. 378,379
Chem. Zentralbl., 1936 , vol. 107, # I p. 1622
反应条件
potassium hydroxide; bromine
zuletzt unter Erwaermen;
参考文献
Brydowna; Wiszniewski
Roczniki Chemii, 1935 , vol. 15, p. 378,379
Chem. Zentralbl., 1936 , vol. 107, # I p. 1622
