2-苯基-1,3-二恶烷合成路线 （共 72 条）
反应条件
[Pd(SiPr2)Cl2]2; potassium tert-butylate; oxygen; isopropyl alcohol; (-)-sparteine
T=50°C; regioselective reaction;
参考文献
Gligorich, Keith M.; Iwai, Yasumasa; Cummings, Sarah A.; Sigman, Matthew S.
Tetrahedron, 2009 , vol. 65, # 26 p. 5074 - 5083
反应条件
trifluorormethanesulfonic acid
T=100°C; 12 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Fukuzawa, Shin-Ichi; Tsuchimoto, Teruhisa; Hiyama, Tamejiro
Journal of Organic Chemistry, 1997 , vol. 62, # 1 p. 151 - 156
反应条件
trifluorormethanesulfonic acid
T=110°C; 7 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Fukuzawa, Shin-Ichi; Tsuchimoto, Teruhisa; Hiyama, Tamejiro
Journal of Organic Chemistry, 1997 , vol. 62, # 1 p. 151 - 156
反应条件
tetrachlorosilane in dichloromethane
T=20°C; Transdithioacetalization; 0.5 h;
参考文献
Firouzabadi, Habib; Iranpoor, Nasser; Karimi, Babak; Hazarkhani, Hassan
Synlett, 2000 , # 2 p. 263 - 265
反应条件
in dichloromethane
T=20°C; 3 h;
参考文献
Chalova, O. B.; Kurmaeva, E. S.; Kantor, E. A.; Kiladze, T. K.; Rakhmankulov, D. L.
Journal of Organic Chemistry USSR (English Translation), 1982 , vol. 18, p. 1434 - 1437
Zhurnal Organicheskoi Khimii, 1982 , vol. 18, # 8 p. 1640 - 1644
反应条件
1: Al-MCM-41 (Si/Al = 48) / dichloromethane / 2 h / 30 °C / Inert atmosphere
2: hydrogenchloride; water / methanol / 0.5 h / 20 °C
3: dipyridinium dichromate / dichloromethane / 14 h / 20 °C / Molecular sieve
4: potassium hydroxide / methanol; water / 14 h / 20 °C
View Scheme
参考文献
Ito, Suguru; Hayashi, Akira; Komai, Hirotomo; Yamaguchi, Hitoshi; Kubota, Yoshihiro; Asami, Masatoshi
Tetrahedron, 2011 , vol. 67, # 11 p. 2081 - 2089
反应条件
trifluorormethanesulfonic acid
T=100°C; 12 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Fukuzawa, Shin-Ichi; Tsuchimoto, Teruhisa; Hiyama, Tamejiro
Journal of Organic Chemistry, 1997 , vol. 62, # 1 p. 151 - 156
反应条件
aluminum oxide; Oxonereg;; water in chloroform
T=50°C; 3 h;
参考文献
Curini, Massimo; Epifano, Francesco; Marcotullio, Maria Carla; Rosati, Ornelio
Synlett, 1999 , # 6 p. 777 - 779
反应条件
aluminum oxide; oxone in chloroform
T=50°C; 2 h; Product distribution; Further Variations:ReagentsSolventsTemperatures;
参考文献
Akbalina; Zlotskii; Kabal'nova; Grigor'ev; Kotlyar; Shereshovets
Russian Journal of Applied Chemistry, 2002 , vol. 75, # 7 p. 1120 - 1122
反应条件
2,2'-azo-bisisobutyronitrile; chloroform in benzene
5 h; Heating;
参考文献
Hai-Xia, Lin; Liang-Heng, Xu; Nai-Ju, Huang
Synthetic Communications, 1997 , vol. 27, # 2 p. 303 - 306
