2-苯基-1,3-二恶烷合成路线 （共 72 条）
反应条件
acetyl chloride in methanol T=20°C; 3 h; Green chemistry; chemoselective reaction;
参考文献
Yu, Hai-Feng
Synthetic Communications, 2013 , vol. 43, # 9 p. 1280 - 1286
反应条件
lithium trifluoromethane sulfonate T=90°C; 1 h;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 74, # 12 p. 2401 - 2406
反应条件
acetyl chloride in methanol T=20°C; 3 h; Green chemistry; chemoselective reaction;
参考文献
Synthetic Communications, , vol. 43, # 9 p. 1280 - 1286
反应条件
acetyl chloride in methanol 0.5 h; RefluxGreen chemistry; TemperatureTime; chemoselective reaction;
参考文献
Synthetic Communications, , vol. 43, # 9 p. 1280 - 1286
反应条件
1: 71 percent / LiAlH4, AlCl3 / diethyl ether / 4 h / Heating 2: triethylamine / 0.25 h / 0 °C 3: LiBr / acetone / Heating View Scheme
参考文献
Canadian Journal of Chemistry, , vol. 74, # 12 p. 2487 - 2502
反应条件
trifluorormethanesulfonic acid 10 h; Heating;
参考文献
Journal of Organic Chemistry, , vol. 62, # 1 p. 151 - 156
反应条件
1: 71 percent / LiAlH4, AlCl3 / diethyl ether / 4 h / Heating 2: triethylamine / 0.25 h / 0 °C 3: LiBr / acetone / Heating 4: 71 percent / NaH, n-butyllithium / tetrahydrofuran; hexane / 3 h / Ambient temperature View Scheme
参考文献
Tokoroyama, Takashi; Kusaka, Hisashi
Canadian Journal of Chemistry, 1996 , vol. 74, # 12 p. 2487 - 2502
反应条件
lithium aluminium tetrahydride; aluminium trichloride in diethyl ether 2 h; Ambient temperature;
参考文献
Kozikowski, Alan P.; Stein, Philip D.
Journal of Organic Chemistry, 1984 , vol. 49, # 13 p. 2301 - 2309
反应条件
trimethylsilyl trifluoromethanesulfonate; dimethylsulfide borane complex in dichloromethane
参考文献
Zhang, Yin-Jie; Dayoub, Wissam; Chen, Guo-Rong; Lemaire, Marc
Green Chemistry, 2011 , vol. 13, # 10 p. 2737 - 2742
反应条件
lithium aluminium tetrahydride; zirconium tetrachloride in diethyl ether T=30°C; 12 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Shaozu, Wu; Yulan, Zhang; Tianhui, Ren
Gazzetta Chimica Italiana, 1991 , vol. 121, # 9 p. 445 - 447
