反应条件
catalyst: charcoal in neat (no solvent) continous process, three reaction chambers (loaded with charcoal as catalyst); 160-180°C (first chamber/formation of SOCl2, COCl2, SO2Cl2, CO2), 180-220°C (second/decompn. of SO2Cl2 and same products), 280-350°C (third/SOCl2, CO2);;
参考文献
S: MVol.B3, 122, page 1791 - 1793
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C. A., , p. 7201
US2471946 , ;
C. I, , p. 772