2-甲基-2-丙基(3-氨基-3-亚氨基丙基)氨基甲酸酯合成路线 （共 4 条）
反应条件
ammonia in isopropyl alcohol
1.) warming, 30 min, 2.) reflux, 12 h;
参考文献
Barker, Peter L.; Gendler, Paul L.; Rapoport, Henry
Journal of Organic Chemistry, 1981 , vol. 46, # 12 p. 2455 - 2465
反应条件
1: 91 percent / NaOH / H2O; diethyl ether / 12 h
2: 85 percent / H2S, diethylamine / dimethylformamide / 3.5 h / 55 °C
3: 89 percent / CH2Cl2 / 12 h / Heating
4: 96 percent / 1.) NH3 / propan-2-ol / 1.) warming, 30 min, 2.) reflux, 12 h
View Scheme
参考文献
Barker, Peter L.; Gendler, Paul L.; Rapoport, Henry
Journal of Organic Chemistry, 1981 , vol. 46, # 12 p. 2455 - 2465
反应条件
1: 85 percent / H2S, diethylamine / dimethylformamide / 3.5 h / 55 °C
2: 89 percent / CH2Cl2 / 12 h / Heating
3: 96 percent / 1.) NH3 / propan-2-ol / 1.) warming, 30 min, 2.) reflux, 12 h
View Scheme
参考文献
Barker, Peter L.; Gendler, Paul L.; Rapoport, Henry
Journal of Organic Chemistry, 1981 , vol. 46, # 12 p. 2455 - 2465
反应条件
1: 89 percent / CH2Cl2 / 12 h / Heating
2: 96 percent / 1.) NH3 / propan-2-ol / 1.) warming, 30 min, 2.) reflux, 12 h
View Scheme
参考文献
Barker, Peter L.; Gendler, Paul L.; Rapoport, Henry
Journal of Organic Chemistry, 1981 , vol. 46, # 12 p. 2455 - 2465
