3-(三甲基硅基)乙炔基苯甲醛合成路线 （共 5 条）
反应条件
copper(l) iodide; bis(benzonitrile)palladium(II) dichloride; tri-tert-butyl phosphine; diisopropylamine in 1,4-dioxane Inert atmosphere;
参考文献
De Miguel, Gustavo; Wielopolski, Mateusz; Schuster, David I.; Fazio, Michael A.; Lee, Olivia P.; Haley, Christopher K.; Ortiz, Angy L.; Echegoyen, Luis; Clark, Timothy; Guldi, Dirk M.
Journal of the American Chemical Society, 2011 , vol. 133, # 33 p. 13036 - 13054
反应条件
triphenylphosphine in triethylamine
参考文献
Vicente, Maria da Graca Henriques; Marzilli, Luigi G.
Patent: US2004/116385 A1, 2004 ;
反应条件
piperidine; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide in tetrahydrofuran Sonogashira coupling; Inert atmosphere;
参考文献
Molina-Ontoria, Agustin; Fernandez, Gustavo; Wielopolski, Mateusz; Atienza, Carmen; Sanchez, Luis; Gouloumis, Andreas; Clark, Timothy; Martin, Nazario; Guldi, Dirk M.
Journal of the American Chemical Society, 2009 , vol. 131, # 34 p. 12218 - 12229
反应条件
1: With potassium fluoride in methanol T=22°C; 6 h; 2: With sodium tetrahydroborate in methanol T=0°C; 0.5 h;
参考文献
PFIZER INC.
Patent: WO2004/63198 A1, 2004 ;
Location in patent: Page 121 ;
WO 2004/063198 A1
反应条件
methanol; potassium carbonate in tetrahydrofuran Inert atmosphere;
参考文献
Molina-Ontoria, Agustin; Fernandez, Gustavo; Wielopolski, Mateusz; Atienza, Carmen; Sanchez, Luis; Gouloumis, Andreas; Clark, Timothy; Martin, Nazario; Guldi, Dirk M.
Journal of the American Chemical Society, 2009 , vol. 131, # 34 p. 12218 - 12229
