反应条件
1: sulfuric acid / 0.25 h / 130 °C / Cooling with ice
2: potassium carbonate / acetone / Inert atmosphere; Reflux
3: selenium(IV) oxide / 1,4-dioxane / 5 h / 180 °C / Inert atmosphere; Sealed tube
4: n-butyllithium; triphenyl-methyl-phosphonium iodide / tetrahydrofuran / 3 h / -78 - 20 °C / Inert atmosphere
5: sodium acetate; palladium diacetate / acetonitrile / 0.17 h
View Scheme
参考文献
Soldi, Cristian; Moro, Angelica V.; Pizzolatti, Moacir G.; Correia, Carlos R. D.
European Journal of Organic Chemistry, 2012 , # 19 p. 3607 - 3616
