in n-heptane byproducts: CH3C6H5; under purified Ar atm.; soln. of TiCl4 in heptane added to soln. of Ti(η6-MeC6H5)2 in heptane; mixt. stirred for 18 h at room temp.; solid filtered; washed (heptane); dried (vac.); elem. anal.;
参考文献
Calderazzo, Fausto; Englert, Ulli; Pampaloni, Guido; Volpe, Manuel
Journal of Organometallic Chemistry, 2005 , vol. 690, # 14 p. 3321 - 3332
hydrogen in gas byproducts: HCl; Irradiation (UV/VIS); in a laser powder synthesis cell; 1100°C; X-ray diffraction; transmission electron microscopy; single point BET surface area analysis; thermal gravimetric analysis; differential thermalanalysis; atomic absorption spectroscopy;
参考文献
Casey; Haggerty
Journal of Materials Science, 1987 , vol. 22, # 2 p. 737 - 744
