反应条件
in neat (no solvent)
byproducts: OF2; introduction of F2 into steel chamber, sulfur in compartments; detailed description of apparatus and handling given;; first passing through Ni (or Monel) tube (400°C); second Cu column (H2O sprayed); passed into steel column (containing carbon/Fe shavings; aq. NaOH sprayed); dried in column (containing solid NaOH, BaO or P2O5);;
参考文献
Schumb, W. C.
Industrial and Engineering Chemistry, 1947 , vol. 39, p. 421 - 423
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Gmelin Handbook: S: MVol.B3, 83, page 1712 - 1714
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Schumb, W. C.
Inorganic syntheses, Bd. 3, New York 1950, S. 119/123
