bromine in tetrachloromethane
byproducts: NH4Br; heating of S with excess Br2 in sealed vessel (vac., 50°C, 24 h),addn. of CCl4, bubbling NH3 through soln. to pH=8; filtration off of NH4Br, TLC (SiO2, CCl4);
参考文献
Apter, S.; Carruthers, M.; Sutcliffe, L. H.
Inorganica Chimica Acta, 1978 , vol. 31, p. L455 - L456
Pinkerton,A.A.; Cavell,R.G.
Journal of the American Chemical Society, 1972 , vol. 94, p. 1870 - 1874
View citing articles Show Details
Gmelin Handbook: F: PerFHalOrg.3, 1.12, page 137 - 160
at 225°C, under pressure; at 200°C in presence of iodine;
参考文献
Krespan,C.G.
Journal of the American Chemical Society, 1961 , vol. 83, p. 3434 - 3437
View citing articles Show Details
Gmelin Handbook: F: PerFHalOrg.1, 1.1.5.2, page 57 - 85
at 225°C under pressure; at 200°C in presence of iodine;
参考文献
Krespan,C.G. et al.
Journal of the American Chemical Society, 1960 , vol. 82, p. 1515 - 1516
View citing articles Show Details
Gmelin Handbook: F: PerFHalOrg.1, 1.1.5.2, page 57 - 85
