at 120°C, 0.5-0.9 Torr, continuous method in a quartz tube with high-voltage discharge;
参考文献
Schenk, P. W.; Holst, W.
Zeitschrift fuer Anorganische und Allgemeine Chemie, 1963 , vol. 319, p. 337 - 349
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Gmelin Handbook: S: SVol.3, 1.10.1, page 17 - 21
Schenk, P. W.; Holst, W.
Zeitschrift fuer Anorganische und Allgemeine Chemie, 1963 , vol. 319, p. 337 - 349
Full Text Show Details
Gmelin Handbook: S: SVol.3, 1.18.5.3, page 64 - 65
silver(I) in ammonia
removal of S(2-) by AgI (formation of Ag2S); filtration; evapn. and heating filtrate (2h/100°C);; evapn. (over H2SO4); extraction (CS2); evapn.;;
参考文献
Ruff, O.; Geisel, E.
Ber., 1905 , vol. 38, p. 2659 - 2667
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Gmelin Handbook: S: MVol.B3, 4, page 1537 - 1540
in ammonia
condensing liquid NH3 on solid sulphur, dissoln. within 1 d (handling of solns. in the dark under high vac., -35°C); investigation of equilibrium by EMF-measurements and light absorption spectra; discussion of photosensitive intermediates;; not isolated;;
参考文献
Prestel, H.; Seelert, S.; Schindewolf, U.
Zeitschrift fuer Physikalische Chemie (Muenchen, Germany), 1986 , vol. 148, p. 97 - 104
