in neat (no solvent) introduction of Cl2O into cooled (-12°C) suspension of S in S2Cl2;; fractionation;;
参考文献
Wurtz, A.
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1866 , vol. 62, p. 460 - 462
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catalyst: C6Cl6 in neat (no solvent) react. in a evacuated silica tube that is in an evacuated silica jacket too at 1180°C for 5-7 d; opening in air, X-ray powder diffraction detn.;
参考文献
Ziebarth, Robin P.; Vassiliou, John K.; Disalvo, F. J.
Journal of the Less-Common Metals, 1989 , vol. 156, p. 207 - 212
in neat (no solvent) heating of equimolar amount in closed tube to 200°C for 6 h;; fractional distillation;;
参考文献
Baroni, A.
Atti della Accademia Nazionale dei Lincei, Classe di Scienze Fisiche, Matematiche e Naturali, Rendiconti, 1937 , vol. 25, p. 722 - 722
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Gmelin Handbook: Se: MVol.B, 89, page 192 - 194
Alexejew, W.
Annalen der Physik (Weinheim, Germany), 1886 , vol. 28, p. 305 - 338
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Gmelin Handbook: S: MVol.A3, 6.10, page 758 - 759
at 225°C, under pressure; at 200°C in presence of iodine;
参考文献
Krespan,C.G.
Journal of the American Chemical Society, 1961 , vol. 83, p. 3434 - 3437
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Gmelin Handbook: F: PerFHalOrg.1, 1.1.5.2, page 57 - 85
