2,6-双(溴甲基)吡啶合成路线 （共 27 条）
反应条件
dimethyl selenoxide in 1,2-dichloro-ethane 4 h; Heating;
参考文献
Syper; Mlochowski
Synthesis, 1984 , vol. NO. 9, p. 747 - 752
反应条件
sodium; tetraphenylethylene in tetrahydrofuran T=-90°C; 288 h;
参考文献
Stephan, Holger; Krueger-Rambusch, Torsten; Gloe, Rarsten; Hasse, Wolfgang; Ahlers, Benedikt; Cammann, Karl; Rissanen, Kari; Brodesser, Gisela; Voegtle, Fritz
Chemistry - A European Journal, 1998 , vol. 4, # 3 p. 434 - 440
反应条件
potassium carbonate; ethanethioamide in N,N-dimethyl-formamide T=55°C; 2 h; further reagents: Li2CO3, Na2CO3, Rb2CO3, Cs2CO3; Product distribution;
参考文献
Voegtle, Fritz; Ley, Fritz
Chemische Berichte, 1983 , vol. 116, # 8 p. 3000 - 3002
反应条件
(i) Na2S*9H2O, EtOH, (ii) O2; Multistep reaction;
参考文献
Galuszko,K.
Roczniki Chemii, 1975 , vol. 49, p. 1597 - 1602
参考文献
Ziessel, Raymond
Tetrahedron Letters, 1989 , vol. 30, # 4 p. 463 - 466
反应条件
potassium carbonate in acetonitrile
Inert atmosphereReflux;
参考文献
Carvalho, Joao F. S.; Louvel, Julien; Doornbos, Maarten L. J.; Klaasse, Elisabeth; Yu, Zhiyi; Brussee, Johannes; Ijzerman, Adriaan P.
Journal of Medicinal Chemistry, 2013 , vol. 56, # 7 p. 2828 - 2840
反应条件
potassium hydroxide in ethanol
5 h; Heating;
参考文献
Ohm, Christian; Breitmaier, Eberhard
Journal fuer Praktische Chemie/Chemiker-Zeitung, 1994 , vol. 336, # 6 p. 530 - 533
反应条件
potassium hydroxide in N,N-dimethyl-formamide
Addition; 0.0833333 h; Heating;
参考文献
Elwahy, Ahmed H. M.; Abbas, Ashraf A.
Tetrahedron, 2000 , vol. 56, # 6 p. 885 - 895
反应条件
Williamson condensation; Inert atmosphere;
参考文献
De Luna, Sara Luisa Rodriguez; Garza, Luis Angel; Bernes, Sylvain; Elizondo, Perla; Najera, Blanca; Perez, Nancy
Polyhedron, 2010 , vol. 29, # 9 p. 2048 - 2052
反应条件
sodium hydride in tetrahydrofuran
Heating;
参考文献
Uiterwijk, Jos W. H. M.; Staveren, Catherina J.van; Reinhoudt, David N.; Hertog, Herman J. den; Kruise, Laminus; Harkema, Sybolt
Journal of Organic Chemistry, 1986 , vol. 51, # 9 p. 1575 - 1587
