丁氧基羰基-D-5-溴尿嘧啶合成路线 （共 4 条）
反应条件
palladium 10 on activated carbon; hydrogen in ethanol P=2585.81 Torr;
参考文献
Qu, Wenchao; Zha, Zhihao; Ploessl, Karl; Lieberman, Brian P.; Zhu, Lin; Wise, David R.; Thompson, Craig B.; Kung, Hank F.
Journal of the American Chemical Society, 2011 , vol. 133, # 4 p. 1122 - 1133
反应条件
sodium hydroxide in 1,4-dioxane; water 24 h; Ambient temperature;
参考文献
European Journal of Medicinal Chemistry, , vol. 27, # 9 p. 899 - 907
反应条件
1: boron trifluoride diethyl etherate / dichloromethane; cyclohexane 2: palladium 10 on activated carbon; hydrogen / ethanol / 2585.81 Torr View Scheme
参考文献
Journal of the American Chemical Society, , vol. 133, # 4 p. 1122 - 1133
反应条件
1: 1.) triethylamine, ethyl chloroformate, 2.) sodium borohydride / 1.) THF, RT, 30 min, 2.) water, RT, 4 h 2: 91 percent / carbon tetrabromide, triphenylphosphine / CH2Cl2 / 2 h / Ambient temperature View Scheme
参考文献
Salituro, Gino M.; Townsend, Craig A.
Journal of the American Chemical Society, 1990 , vol. 112, # 2 p. 760 - 770
