4-氨基-2-(甲基硫代)嘧啶-5-腈合成路线 （共 13 条）
反应条件
N-ethyl-N,N-diisopropylamine in N,N-dimethyl-formamide T=0 - 20°C;
参考文献
Synthetic Communications, , vol. 36, # 20 p. 2963 - 2973
反应条件
1: m-chloroperbenzoic acid / tetrahydrofuran / 0 - 20 °C 2: tetrahydrofuran / Heating View Scheme
参考文献
Katiyar, Sanjay Babu; Kumar, Arun; Chauhan, Prem M. S.
Synthetic Communications, 2006 , vol. 36, # 20 p. 2963 - 2973
反应条件
1: m-chloroperbenzoic acid / tetrahydrofuran / 0 - 20 °C 2: tetrahydrofuran / Heating View Scheme
参考文献
Katiyar, Sanjay Babu; Kumar, Arun; Chauhan, Prem M. S.
Synthetic Communications, 2006 , vol. 36, # 20 p. 2963 - 2973
反应条件
1: With diisobutylaluminium hydride in tetrahydrofuran; dichloromethane T=0°C; 2.5 h; 2: With hydrogenchloride in tetrahydrofuran; dichloromethane; water
参考文献
IRM LLC
Patent: WO2005/34869 A2, 2005 ;
Location in patent: Page/Page column 31 ;
WO 2005/034869 A2
反应条件
1: m-chloroperbenzoic acid / tetrahydrofuran / 0 - 20 °C 2: tetrahydrofuran / Heating View Scheme
参考文献
Katiyar, Sanjay Babu; Kumar, Arun; Chauhan, Prem M. S.
Synthetic Communications, 2006 , vol. 36, # 20 p. 2963 - 2973
反应条件
1: m-chloroperbenzoic acid / tetrahydrofuran / 0 - 20 °C
2: tetrahydrofuran / Heating
3: t-BuOK / dimethylformamide / 0 - 20 °C
View Scheme
参考文献
Katiyar, Sanjay Babu; Kumar, Arun; Chauhan, Prem M. S.
Synthetic Communications, 2006 , vol. 36, # 20 p. 2963 - 2973
反应条件
1: m-chloroperbenzoic acid / tetrahydrofuran / 0 - 20 °C
2: tetrahydrofuran / Heating
3: t-BuOK / dimethylformamide / 0 - 20 °C
View Scheme
参考文献
Katiyar, Sanjay Babu; Kumar, Arun; Chauhan, Prem M. S.
Synthetic Communications, 2006 , vol. 36, # 20 p. 2963 - 2973
反应条件
1: m-chloroperbenzoic acid / tetrahydrofuran / 0 - 20 °C
2: tetrahydrofuran / Heating
3: t-BuOK / dimethylformamide / 0 - 20 °C
View Scheme
参考文献
Katiyar, Sanjay Babu; Kumar, Arun; Chauhan, Prem M. S.
Synthetic Communications, 2006 , vol. 36, # 20 p. 2963 - 2973
反应条件
1: m-chloroperbenzoic acid / tetrahydrofuran / 0 - 20 °C
2: tetrahydrofuran / Heating
3: t-BuOK / dimethylformamide / 0 - 20 °C
View Scheme
参考文献
Katiyar, Sanjay Babu; Kumar, Arun; Chauhan, Prem M. S.
Synthetic Communications, 2006 , vol. 36, # 20 p. 2963 - 2973
反应条件
1: m-chloroperbenzoic acid / tetrahydrofuran / 0 - 20 °C
2: tetrahydrofuran / Heating
3: t-BuOK / dimethylformamide / 0 - 20 °C
View Scheme
参考文献
Katiyar, Sanjay Babu; Kumar, Arun; Chauhan, Prem M. S.
Synthetic Communications, 2006 , vol. 36, # 20 p. 2963 - 2973
