3-吡咯烷-2-丙烷-1-醇合成路线 （共 7 条）
反应条件
hydrogen; 5-palladium/activated carbon in ethanol
T=35°C; P=760.051 Torr; 8 h;
参考文献
Nippon Shinyaku Co., Ltd.
Patent: EP1400518 A1, 2004 ;
Location in patent: Page 23 ;
反应条件
lithium aluminium tetrahydride in tetrahydrofuran
Ambient temperature;
参考文献
Wagner, Barbara J.; Doi, Joyce Takahashi; Musker, W. Kenneth
Journal of Organic Chemistry, 1990 , vol. 55, # 13 p. 4156 - 4162
反应条件
sodium tetrahydroborate in ethanol
48 h;
参考文献
Provot, Olivier; Celerier, Jean-Pierre; Lhommet, Gerard
Journal of Heterocyclic Chemistry, 1998 , vol. 35, # 2 p. 371 - 376
反应条件
di-tert-butyl peroxide
T=120 - 122°C; unter Druck;
参考文献
Urry; Juveland
Journal of the American Chemical Society, 1958 , vol. 80, p. 3322,3326
反应条件
1: 76.3 percent / H2 / platinum oxide / methanol / 52 h / 23 °C / 2280 Torr
2: 70.3 percent / lithium aluminum hydride / tetrahydrofuran / Ambient temperature
View Scheme
参考文献
Wagner, Barbara J.; Doi, Joyce Takahashi; Musker, W. Kenneth
Journal of Organic Chemistry, 1990 , vol. 55, # 13 p. 4156 - 4162
参考文献
Urry; Juveland
Journal of the American Chemical Society, 1958 , vol. 80, p. 3322,3326
反应条件
1: 65 percent / NaHCO3 / H2O / 1.5 h / Ambient temperature
2: 86 percent / PCC / CH2Cl2 / 3 h / Ambient temperature
3: 55 percent / ammonium formate / Pd/C / methanol / 0.5 h / Heating
View Scheme
参考文献
Provot, Olivier; Celerier, Jean-Pierre; Lhommet, Gerard
Journal of Heterocyclic Chemistry, 1998 , vol. 35, # 2 p. 371 - 376
