4-溴-3,5-二甲基苯甲酸合成路线 (共 4 条)
反应条件
lithium aluminium tetrahydride in diethyl ether
参考文献
Grisdale,P.J. et al.
Journal of Organic Chemistry, 1971 , vol. 36, p. 544 - 549
反应条件
1,3-bis-(diphenylphosphino)propane; 1,1,1,3,3,3-hexamethyl-disilazane; palladium dichloride in methanol T=80°C; 4.167 h;
参考文献
Breslin, Henry J.; Cai, Chaozhong; He, Wei; Kavash, Robert W.
Patent: US2005/203143 A1, 2005 ;
Location in patent: Page/Page column 45 ;
US 20050203143 A1
反应条件
thionyl chloride Behandeln des erhaltenen Saeurechlorids mit wss. Ammoniak;
参考文献
Spitzer; Wheland
Journal of the American Chemical Society, 1940 , vol. 62, p. 2995,3001
反应条件
1: thionyl chloride / Behandeln des erhaltenen Saeurechlorids mit wss. Ammoniak 2: phosphorus (V)-chloride View Scheme
参考文献
Spitzer; Wheland
Journal of the American Chemical Society, 1940 , vol. 62, p. 2995,3001