3-氨基-N-羟基-吡嗪羧胺合成路线 （共 18 条）
反应条件
hydroxylamine in methanol
75 h; Ambient temperature;
参考文献
Kocevar, Marjan; Stanovnik, Branko; Tisler, Miha
Tetrahedron, 1983 , vol. 39, # 5 p. 823 - 829
参考文献
Kocevar, Marjan; Stanovnik, Branko; Tisler, Miha
Heterocycles, 1981 , vol. 15, # 1 p. 293 - 296
反应条件
1: 80 percent / NH2OH*HCl / ethanol / 0.67 h / Heating
2: H2O / 7 h / Heating
View Scheme
参考文献
Kocevar, Marjan; Stanovnik, Branko; Tisler, Miha
Heterocycles, 1981 , vol. 15, # 1 p. 293 - 296
反应条件
1: 68 percent / 3.5 h / 105 °C
2: hydroxylamine / methanol / 75 h / Ambient temperature
View Scheme
参考文献
Kocevar, Marjan; Stanovnik, Branko; Tisler, Miha
Tetrahedron, 1983 , vol. 39, # 5 p. 823 - 829
反应条件
acetic acid
0.833333 h; Heating;
参考文献
Kocevar, M.; Stanovnik, B.; Tisler, M.
Journal of Heterocyclic Chemistry, 1982 , vol. 19, p. 1397 - 1402
反应条件
1: 9 percent / methanol / 4 h / Ambient temperature
2: 1.) water, reflux, 7 h, 2.) MeOH, reflux, 1 min
View Scheme
参考文献
Kocevar, Marjan; Stanovnik, Branko; Tisler, Miha
Tetrahedron, 1983 , vol. 39, # 5 p. 823 - 829
反应条件
1: 80 percent
2: H2O / 7 h / Heating
3: 50 percent / 15 h / Heating
4: 87 percent / NH3 / methanol / 24 h / Ambient temperature
View Scheme
参考文献
Kocevar, Marjan; Stanovnik, Branko; Tisler, Miha
Heterocycles, 1981 , vol. 15, # 1 p. 293 - 296
反应条件
1: 80 percent
2: H2O / 7 h / Heating
3: 50 percent / acetic acid / 3 h
View Scheme
参考文献
Kocevar, Marjan; Stanovnik, Branko; Tisler, Miha
Heterocycles, 1981 , vol. 15, # 1 p. 293 - 296
