(2S)-2-[(四氢-2H-吡喃-2-基)氧基]-1-丙醇合成路线 （共 8 条）
反应条件
lithium aluminium tetrahydride in diethyl ether 0 deg C, 165 min; reflux 2 h;
参考文献
Brunsveld; Zhang; Glasbeek; Vekemans; Meijer
Journal of the American Chemical Society, 2000 , vol. 122, # 26 p. 6175 - 6182
反应条件
1: 94 percent / TsOH*Py / CH2Cl2 / 2 h / 25 °C 2: 97 percent / lithium aluminium hydride / diethyl ether / 1.5 h / 25 °C View Scheme
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 26, # 9.1 p. 1613 - 1616
Zhurnal Organicheskoi Khimii, , vol. 26, # 9 p. 1864 - 1869
反应条件
lithium aluminium tetrahydride in diethyl ether T=0°C; Reflux;
参考文献
Pfukwa, Rueben; Kouwer, Paul H. J.; Rowan, Alan E.; Klumperman, Bert
Angewandte Chemie - International Edition, 2013 , vol. 52, # 42 p. 11040 - 11044
Angewandte Chemie, 2013 , vol. 125, # 42 p. 11246 - 11250,5
反应条件
lithium aluminium tetrahydride in diethyl ether
参考文献
Neubert, M. E.; Sabol-Keast, S.
Molecular Crystals and Liquid Crystals (1969-1991), 1990 , vol. 188, # 1 p. 67 - 74
反应条件
lithium aluminium tetrahydride in diethyl ether
参考文献
Synthetic Communications, , vol. 23, # 15 p. 2159 - 2169
反应条件
hydrogenchloride in methanol 12 h;
参考文献
Cooper, Keith D.; Walborsky, Harry M.
Journal of Organic Chemistry, 1981 , vol. 46, # 10 p. 2110 - 2116
反应条件
Dowex 50 X 8 (H+); ammonia; sodium hydride 1.) mineral oil, DMF, 0 deg C, 1 h; room temperature, 48 h, 2.) MeOH, 2 h, 3.) 70percent aq. MeOH, reflux, 4 h; Yield given. Multistep reaction;
参考文献
Collection of Czechoslovak Chemical Communications, , vol. 60, # 8 p. 1390 - 1409
反应条件
Dowex 50 X 8 (H+); ammonia; sodium hydride 1.) mineral oil, DMF, 0 deg C, 1 h; room temperature, 48 h, 2.) MeOH, 2 h, 3.) 70percent aq. MeOH, reflux, 4 h; Yield given. Multistep reaction;
参考文献
Collection of Czechoslovak Chemical Communications, , vol. 60, # 8 p. 1390 - 1409
