2-[(二甲基氨基)甲基]环己酮合成路线 （共 38 条）
参考文献
Nasarow; Saw'jalow
Zhurnal Obshchei Khimii, 1955 , vol. 25, p. 508,514; engl. Ausg. S. 477, 481
反应条件
sodium hydroxide
6 h; Heating; Yield given;
参考文献
Black, David St. C.; Johnstone, Lynn M.
Australian Journal of Chemistry, 1984 , vol. 37, # 1 p. 117 - 128
反应条件
ethanol; dimethyl sulfate
und anschliessenden Erwaermen mit Phthalimid und Natriumaethylat in Aethanol;
参考文献
Farbenfabr.Bayer
Patent: DE933339 , 1954 ;
反应条件
1: ethanolic sodium ethylate
2: ethanolic KOH-solution / Erhitzen des Reaktionsprodukts
View Scheme
参考文献
Mannich; Koch
Chemische Berichte, 1942 , vol. 75, p. 803
反应条件
1: aqueous K2CO3
2: sulfur
3: sulfur
View Scheme
参考文献
Grandberg et al.
Zhurnal Obshchei Khimii, 1959 , vol. 29, p. 2537,2540; engl. Ausg. S. 2499, 2502
参考文献
Gill et al.
Journal of the American Chemical Society, 1952 , vol. 74, p. 4923,4927
反应条件
sodium hydroxide in water
T=96 - 98°C; 5 h; Yield given;
参考文献
Akimova, T. I.; Kosenko, S. V.; Tilichenko, M. N.
Journal of Organic Chemistry USSR (English Translation), 1991 , vol. 27, # 12 p. 2271 - 2277
Zhurnal Organicheskoi Khimii, 1991 , vol. 27, # 12 p. 2553 - 2560
反应条件
sodium hydroxide in water
T=90 - 100°C; 5 h; Further byproducts given;
参考文献
Akimova, T. I.; Kosenko, S. V.; Tilichenko, M. N.
Journal of Organic Chemistry USSR (English Translation), 1991 , vol. 27, # 12 p. 2271 - 2277
Zhurnal Organicheskoi Khimii, 1991 , vol. 27, # 12 p. 2553 - 2560
