2-甲基-1-苯基-丙-2-烯-1-酮合成路线 （共 105 条）
反应条件
pyridine; triethylamine; benzene
参考文献
Stevens; Ettling
Journal of the American Chemical Society, 1955 , vol. 77, p. 5412
反应条件
in methanol-d4
T=-50°C;
参考文献
Reich,H.J.; Hoeger,C.A.; Willis,W.W.
Journal of the American Chemical Society, 1982 , vol. 104, p. 2936
反应条件
1: ether BF3
2: quinoline
View Scheme
参考文献
Tilitschenko; Popowa
Zhurnal Obshchei Khimii, 1953 , vol. 23, p. 118,120; engl. Ausg. S. 115
反应条件
1: C11H13PolS2 With n-butyllithium in tetrahydrofuran
T=-35°C; 2 h; solid phase reaction;
2: acetone in tetrahydrofuran; Petroleum ether
T=-10°C; solid phase reaction;
3: With mercury(II) perchlorate; water; calcium carbonate in tetrahydrofuran
参考文献
Bertini, Vincenzo; Lucchesini, Francesco; Pocci, Marco; Alfei, Silvana; Idini, Barbara
Synlett, 2008 , # 8 p. 1141 - 1144
反应条件
2,6-dimethylpyridine
T=100°C; 2.5 h;
参考文献
Creary, Xavier
Journal of the American Chemical Society, 1984 , vol. 106, # 19 p. 5568 - 5577
反应条件
oxalic acid; silica gel; mercury dichloride in dichloromethane; water
15 h; Ambient temperature;
参考文献
Pellet, Michele; Huet, Francois
Tetrahedron, 1988 , vol. 44, # 14 p. 4463 - 4468
反应条件
sodium hydrogencarbonate
参考文献
Hart; Curtis
Journal of the American Chemical Society, 1957 , vol. 79, p. 931
反应条件
triethylamine tris(hydrogen fluoride); triethylamine in acetonitrile
T=80°C; 20 h;
参考文献
Giudicelli; Pica; Veyron
Tetrahedron Letters, 1990 , vol. 31, # 45 p. 6527 - 6530
反应条件
(i) NaIO4, (ii) (heating); Multistep reaction;
参考文献
Reich,H.J.; Renga,J.M.
Journal of the Chemical Society, Chemical Communications, 1974 , p. 135 - 136
反应条件
phosphorous acid trimethyl ester in dichloromethane-d2
T=-91°C; Title compound not separated from byproducts;
参考文献
Reich, Hans J.; Hoeger, Carl A.; Willis, W. W., Jr.
Tetrahedron, 1985 , vol. 41, # 21 p. 4771 - 4780
