2-甲基-1-苯基-丙-2-烯-1-酮合成路线 （共 105 条）
反应条件
palladium diacetate; tris(4-methoxyphenyl)-phosphine
T=60°C; 16 h;
参考文献
Gossen, Lukas J.; Ghosh, K.
Angewandte Chemie, International Edition, 2001 , vol. 40, # 18 p. 3458 - 3460
Angewandte Chemie, 2001 , vol. 40, # 18 p. 3458 - 3468
反应条件
sodium carbonate; palladium diacetate in acetone
T=20°C; Suzuki reaction; 1 h;
参考文献
Korolev; Bumagin
Russian Chemical Bulletin, 2004 , vol. 53, # 2 p. 364 - 369
反应条件
potassium carbonate in tetrahydrofuran
T=70°C; 0.25 h;
参考文献
Villieras, Jean; Rambaud, Monique
Synthesis, 1984 , # 5 p. 406 - 408
反应条件
acetic anhydride
T=80°C; 6 h;
参考文献
Rodrigues, J. Augusto R.; Siqueira-Filho, Ezequias P.; De Mancilha, Moacir; Moran, Paulo J. S.
Synthetic Communications, 2003 , vol. 33, # 2 p. 331 - 340
反应条件
sodium hydroxide; acetic anhydride in dichloromethane
参考文献
Hoechst Celanese Corporation
Patent: US5489712 A1, 1996 ;
反应条件
in diethylene glycol dimethyl ether
T=180°C; 1 h; Inert atmosphere;
参考文献
Amii, Hideki; Oshiro, Kojun; Morimoto, Yoshimichi; Matsuura, Makoto
Patent: US2012/277458 A1, 2012 ;
Location in patent: Page/Page column 10 ;
反应条件
in tetrachloromethane; chloroform
T=65°C; 240 h;
参考文献
Paterson, Ian
Tetrahedron, 1988 , vol. 44, # 13 p. 4207 - 4220
反应条件
sodium acetate
T=95°C; 0.25 h;
参考文献
Suzuki, Takayoshi; Ohwada, Tomohiko; Shudo, Koichi
Journal of the American Chemical Society, 1997 , vol. 119, # 29 p. 6774 - 6780
反应条件
diethylamine in dichloromethane
192 h; Heating;
参考文献
Hon, Yung-Son; Hsu, Tzyy-Rong; Chen, Chun-Yan; Lin, Yi-Hui; Chang, Fong-Jong; Hsieh, Cheng-Han; Szu, Ping-Hui
Tetrahedron, 2003 , vol. 59, # 9 p. 1509 - 1520
反应条件
2: O3
3: tetradeuteriomethanol / -50 °C
View Scheme
参考文献
Reich,H.J.; Hoeger,C.A.; Willis,W.W.
Journal of the American Chemical Society, 1982 , vol. 104, p. 2936
